Cyanamidnatrium → HCID 68525580, compound
Reaction equation
[CH3:1][C:2]1([CH3:19])[CH2:7][CH2:6][CH:5]([C:8]2[CH:18]=[CH:17][C:11]([O:12][CH2:13][CH:14]3[CH2:16][O:15]3)=[CH:10][CH:9]=2)[CH2:4][CH2:3]1.[N:20]#[C:21][NH2:22].[Na]>>[CH3:19][C:2]1([CH3:1])[CH2:3][CH2:4][CH:5]([C:8]2[CH:9]=[CH:10][C:11]([O:12][CH2:13][CH:14]3[O:15][C:21]([NH2:22])=[N:20][CH2:16]3)=[CH:17][CH:18]=2)[CH2:6][CH2:7]1Participants
3
Procedure
The title compound was prepared from 2-[4-(4,4-dimethyl-cyclohexyl)-phenoxymethyl]-oxirane and sodium hydrogen cyanamide according to the procedures employed for the preparation of the compound in Step 2 of Example 1.
Workup
- customemployed for the preparation of the compound in Step 2 of Example 1
Sources & evidence
- ORD record
- ord-9c0a657e75424500932b3bd76eea79a4
- Source dataset
- uspto-grants-2014_02
- Patent number
- US08642603B2
Reaction notes
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