HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methyl-2-cyclohexen-1-one → 3-Methyl-2-cyclohexen-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methyl-2-cyclohexen-1-one | HCID 14511 | — |
| Reactant | HCID 178418373 | HCID 178418373 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 3-Methyl-2-cyclohexen-1-one | HCID 14511 | — |
| Product | Cyclohexanone, 3,3-dimethyl- | HCID 76322 | — |
Reaction Steps
First, 3-methyl-cyclohexenone was prepared in accordance with the procedures of Jirgensons et. al., Euro. J. Med. Chem. 35 (2000) 555-565. Then, 3-methyl-cyclohexenone was reacted with methyl magnesium iodide in the presence of cuprous chloride in diethyl ether to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08642603B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-f2ed5d56b2764e25bcbeb6e69c3a3e53 |
| Source note | uspto-grants-2014_02 |