5-Hexen-1-ol → N-[(Hex-5-en-1-yloxy)carbonyl]-L-norleucine

HRID 2377608Notes

Reaction equation

HRID 2377608 reaction equation
[CH2:1]([O:6][C:7]([NH:9][C@H:10]([C:15]([OH:17])=[O:16])[CH2:11][CH2:12][CH2:13][CH3:14])=[O:8])[CH2:2][CH2:3][CH:4]=[CH2:5].[CH2:18](O)CCCC=C>>[CH2:1]([O:6][C:7]([NH:9][C@H:10]([C:15]([OH:17])=[O:16])[CH2:11][CH2:12][CH2:13][CH3:14])=[O:8])[CH2:2][CH2:3][CH2:4][CH:5]=[CH2:18]

Participants

3

Reactant 2

HCID 699635-Hexen-1-olHCID 45378373N-[(pent-4-en-1-yloxy)carbonyl]-norleucine

Product 1

HCID 59856502N-[(Hex-5-en-1-yloxy)carbonyl]-L-norleucine

Procedure

N-[(Hex-5-en-1-yloxy)carbonyl]-L-norleucine was prepared according to the procedure for N-[(pent-4-en-1-yloxy)carbonyl]-L-norleucine by using 5-hexenol instead of 4-pentenol. LRMS (ESI) m/z 258 [(M+H)+; calcd for C13H24NO4: 258].

Sources & evidence

ORD record
ord-46ab7c5a6eae430fbf7015043edff322
Source dataset
uspto-grants-2008_12
Patent number
US07470664B2

Reaction notes

Loading…