(alphaS)-alpha-Aminocyclohexaneacetic acid → (2S)-Cyclohexyl({[(2,2-dimethylhex-5-en-1-yl)oxy]carbonyl}amino)acetic acid

Participants

Role	Name	HCID	Charge
Reactant	(alphaS)-alpha-Aminocyclohexaneacetic acid	HCID 736848	—
Reactant	2,2-Dimethylhex-5-en-1-ol	HCID 10240821	—
Reactant	3-Methyl-N-{[(pent-4-en-1-yl)oxy]carbonyl}-L-valine	HCID 45379928	—
Product	(2S)-Cyclohexyl({[(2,2-dimethylhex-5-en-1-yl)oxy]carbonyl}amino)acetic acid	HCID 45379612	—

Reaction Steps

(2S)-Cyclohexyl({[(2,2-dimethylhex-5-en-1-yl)oxy]carbonyl}amino)acetic acid was prepared according to the procedure for 3-methyl-N-[(pent-4-enyloxy)carbonyl]-L-valine using (2S)-amino(cyclohexyl)acetic acid and 2,2-dimethylhex-5-en-1-ol. LRMS (ESI) m/z 312.3 [(M+H)+; calcd for C17H30NO4: 312.2].

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US07470664B2
Source dataset	uspto-grants-2008_12
ORD ID	ord-fe626430d6594b38b2149e0e8e10ec4e
Source note	uspto-grants-2008_12