HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Bromo-1-hexene → N-[(Hex-5-en-1-yl)(propan-2-yl)carbamoyl]-3-methyl-L-valine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Bromo-1-hexene | HCID 75906 | — |
| Reactant | 3-Methyl-N-[(pent-4-en-1-yl)(propan-2-yl)carbamoyl]-L-valine | HCID 57692680 | — |
| Product | N-[(Hex-5-en-1-yl)(propan-2-yl)carbamoyl]-3-methyl-L-valine | HCID 59856486 | — |
Reaction Steps
N-{[Hex-5-en-1-yl(isopropyl)amino]carbonyl}-3-methyl-L-valine was prepared according to the procedure described for N-{[isopropyl(pent-4-en-1-yl)amino]carbonyl}-3-methyl-L-valine by using 6-bromo-1-hexene in Step 1. LRMS (ESI) m/z 299 [(M+H)+; calcd for C16H31N2O3; 299.2].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07470664B2 |
| Source dataset | uspto-grants-2008_12 |
| ORD ID | ord-ccdd2b0946aa48288a9e7edd34f5c311 |
| Source note | uspto-grants-2008_12 |