4-tert-Butylphenol → 4-tert-Butylphenyl glycidyl ether, (-)-

HRID 237802Notes

Reaction equation

[C:1]([C:5]1[CH:10]=[CH:9][C:8]([OH:11])=[CH:7][CH:6]=1)([CH3:4])([CH3:3])[CH3:2].[CH2:12]1[O:14][C@@H:13]1[CH2:15]Cl>>[C:1]([C:5]1[CH:6]=[CH:7][C:8]([O:11][CH2:15][C@H:13]2[CH2:12][O:14]2)=[CH:9][CH:10]=1)([CH3:4])([CH3:2])[CH3:3]

Participants

Reactant 2

HCID 73934-tert-Butylphenol

HCID 149428(+)-Epichlorohydrin

Product 1

HCID 7193714-tert-Butylphenyl glycidyl ether, (-)-

Procedure

The title compound was prepared from 4-tert-butyl-phenol and S-epichlorohydrin employing the procedures as set forth in Step 1 of Example 1.

Sources & evidence

ORD record: ord-04ef000cf7ff44118071c166eb5bd834
Source dataset: uspto-grants-2014_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08642603B2

Reaction notes

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