1-Naphthalenemethanamine → HCID 62368325, compound

HRID 2378084Notes

Reaction equation

HRID 2378084 reaction equation
[NH2:1][CH2:2][C:3]1[C:12]2[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=2)[CH:6]=[CH:5][CH:4]=1.[NH:13]([C:15](=[O:20])[C:16](OC)=[O:17])[NH2:14]>CO>[NH:13]([C:15](=[O:20])[C:16]([NH:1][CH2:2][C:3]1[C:12]2[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=2)[CH:6]=[CH:5][CH:4]=1)=[O:17])[NH2:14]

Participants

4

Reactant 2

HCID 83551-NaphthalenemethanamineHCID 11355473Methyl hydrazino(oxo)acetate

Product 1

HCID 62368325HCID 62368325, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent2×

Procedure

1.25 ml 1-aminomethylnaphthalene are added to a solution of 1.0 g methyl hydrazino-oxo-acetate in 10 ml of methanol. The solution is stirred for 16 h at ambient temperature and then some of the methanol is eliminated. The precipitate is separated off, washed with diethyl ether, and dried.

Workup

  1. customThe precipitate is separated off
  2. washwashed with diethyl ether
  3. customdried

Sources & evidence

ORD record
ord-2ed23cf9f90c44a0b2d2e202c25b93bd
Source dataset
uspto-grants-2008_12
Patent number
US07470716B2

Reaction notes

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