돌아가기
Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 237811생성일: 2026년 10월 25일

1-Benzyloxy-4-(3,3,5,5-tetramethyl-cyclohex-1-enyl)-benzene → 4-(3,3,5,5-Tetramethyl-cyclohexyl)-phenol

https://huagongshe.com/reaction/237811

반응식

참여 물질

역할이름HCID투입량
반응물1-Benzyloxy-4-(3,3,5,5-tetramethyl-cyclohex-1-enyl)-benzeneHCID 68525815—
촉매PalladiumHCID 23938—
용매MethanolHCID 887—
용매Ethyl AcetateHCID 8857—
생성물4-(3,3,5,5-Tetramethyl-cyclohexyl)-phenolHCID 6852586396.6%

반응 단계

To 10% Pd/C (0.17 g) under N2 was added 1-benzyloxy-4-(3,3,5,5-tetramethyl-cyclohex-1-enyl)-benzene (1.7 g, 5.3 mmol), prepared by a substantially similar procedure to that of Step 1 of Example 18, in MeOH (15 mL) and EtOAc (15 mL). This mixture was stirred under H2 (1 atm) overnight. The reaction mixture was filtered through celite. The filtrate was concentrated to give the title compound as a white solid (1.19 g).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US08642603B2
출처 데이터셋uspto-grants-2014_02
ORD IDord-8b5b782ad61043aab7f5d69373edc6f7
출처 메모uspto-grants-2014_02