HuagongsheHuagongshe Chemistry Print Report · For research reference only
Beta-Propiolactone → HCID 58838616, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Beta-Propiolactone | HCID 2365 | — |
| Reactant | Delta-Valerolactone | HCID 10953 | — |
| Reactant | 10-Bromo-1-decene | HCID 543384 | — |
| Reactant | HCID 53627781 | HCID 53627781 | — |
| Product | HCID 58838616 | HCID 58838616 | 60% |
Reaction Steps
14.30 g of tetrahydro-3-(9-decenyl)-2H-pyrane-2-one of interest was prepared in the same manner as in Example 1 except that 10.01 g (100.0 mmol) of δ-valerolactone and 26.30 g (110.0 mmol) of 10-bromo-1-decene were used instead of β-propiolactone and allyl amide described in Preparation Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07470768B2 |
| Source dataset | uspto-grants-2008_12 |
| ORD ID | ord-73f58ddae53f419dbddef097b9987aeb |
| Source note | uspto-grants-2008_12 |