HuagongsheHuagongshe Chemistry Print Report · For research reference only
ethyl 3-cyclohexylprop-2-ynoate → HCID 59252488, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | ethyl 3-cyclohexylprop-2-ynoate | HCID 316633 | — |
| Reactant | (S)-5-(4-cyclohexyl-phenoxymethyl)-4,5-dihydro-oxazol-2-ylamine | HCID 66875140 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 59252488 | HCID 59252488 | — |
Reaction Steps
The title compound was prepared from (S)-5-(4-cyclohexyl-phenoxymethyl)-4,5-dihydro-oxazol-2-ylamine and cyclohexyl-propynoic acid ethyl ester (see Example 103) employing the procedure described in Example 100. [α]D25 +17.80 (c 0.5, DMSO)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08642603B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-287eb5caada947d5b627140bf2b53e50 |
| Source note | uspto-grants-2014_02 |