Ethyl chloroformate → HCID 86640236, compound

HRID 237844Notes

Reaction equation

[CH3:1][C:2]([CH3:11])([C:9]#[CH:10])[CH2:3][O:4][Si:5]([CH3:8])([CH3:7])[CH3:6].Cl[C:13]([O:15][CH2:16][CH3:17])=[O:14]>>[CH2:16]([O:15][C:13](=[O:14])[C:10]#[C:9][C:2]([CH3:11])([CH3:1])[CH2:3][O:4][Si:5]([CH3:6])([CH3:8])[CH3:7])[CH3:17]

Participants

Reactant 2

HCID 10928Ethyl chloroformate

HCID 86640237HCID 86640237, compound

Product 1

HCID 86640236HCID 86640236, compound

Procedure

The title compound was prepared from (2,2-dimethyl-but-3-ynyloxy)-trimethyl-silane and ethyl chloroformate in accordance with the procedures of G. Cai et al., Tetrahedron, 2006, (5697-5708).

Sources & evidence

ORD record: ord-e39d5d18d14746ccbc1a62db6f587efd
Source dataset: uspto-grants-2014_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08642603B2

Reaction notes

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