Triethoxysilane → HCID 86605938, compound

Participants

Reaction Conditions

Reaction Steps

After 0.61 g of 4-(trifluoromethyl)benzyl-4-(3-butenyloxy)phenyl sulfone and 20 mg of 10% platinum-active carbon were charged in a reaction vessel, and the inside of the vessel was then filled with nitrogen gas, 2 ml of triethoxysilane was added, and the mixture was then further stirred at 100° C. for 4 hours. After the reaction mixture was cooled to room temperature, 20 ml of toluene was added, and the mixture was filtered through a pad of Celite™. After the filtrate was concentrated, dehydrated ethanol was added to the residue, which was then left still over night. After precipitated crystal was removed by filtration, the filtrate was concentrated, and n-hexane was added to collect precipitated crystal by filtration. The obtained crystal was washed with n-hexane to produce 0.53 g of the desired product.

Provenance & Evidence