HCID 69276010, compound → HCID 69277828, compound

HRID 2378522Notes

Reaction equation

HRID 2378522 reaction equation
[CH3:1][C:2]1[CH:61]=[CH:60][C:5]([CH2:6][C:7]2[CH:12]=[C:11]([O:13][CH2:14][CH2:15][CH2:16][CH2:17][Si:18]([O:25][CH2:26]C)([O:22][CH2:23]C)[O:19][CH2:20]C)[CH:10]=[CH:9][C:8]=2[S:28]([C:31]2[CH:36]=[CH:35][C:34]([O:37][CH2:38][CH2:39][CH2:40][CH2:41][Si:42]([O:49][CH2:50]C)([O:46][CH2:47]C)[O:43][CH2:44]C)=[CH:33][C:32]=2[CH2:52][C:53]2[CH:58]=[CH:57][C:56]([CH3:59])=[CH:55][CH:54]=2)(=[O:30])=[O:29])=[CH:4][CH:3]=1>CO>[CH3:1][C:2]1[CH:61]=[CH:60][C:5]([CH2:6][C:7]2[CH:12]=[C:11]([O:13][CH2:14][CH2:15][CH2:16][CH2:17][Si:18]([O:22][CH3:23])([O:25][CH3:26])[O:19][CH3:20])[CH:10]=[CH:9][C:8]=2[S:28]([C:31]2[CH:36]=[CH:35][C:34]([O:37][CH2:38][CH2:39][CH2:40][CH2:41][Si:42]([O:46][CH3:47])([O:49][CH3:50])[O:43][CH3:44])=[CH:33][C:32]=2[CH2:52][C:53]2[CH:58]=[CH:57][C:56]([CH3:59])=[CH:55][CH:54]=2)(=[O:29])=[O:30])=[CH:4][CH:3]=1

Participants

3

Reactant 1

HCID 69276010HCID 69276010, compound

Product 1

HCID 69277828HCID 69277828, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The compound produced in Example 2 was refluxed with a chloroplatinic catalyst in methanol for 3 hours, and was then concentrated to give the desired product as a maize oily material.

Workup

  1. concentrationwas then concentrated

Sources & evidence

ORD record
ord-ce5889ee2aaa497a8cb931f853408aa6
Source dataset
uspto-grants-2008_12
Patent number
US07470803B2

Reaction notes

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