HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethane, 2-bromo-1,1-diethoxy- → 2-Amino-5-bromopyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethane, 2-bromo-1,1-diethoxy- | HCID 74852 | — |
| Reactant | 6-Bromoimidazo[1,2-a]pyridine | HCID 2795547 | — |
| Product | 2-Amino-5-bromopyridine | HCID 70622 | — |
| Product | 6-Bromoimidazo[1,2-a]pyridine | HCID 2795547 | — |
Reaction Steps
The title compound (Intermediate 91, 3.36 g) was obtained from commercially available bromoacetaldehyde-diethylacetal (4.7 ml, WAKO) and 2-amino-5-bromopyridine (4.32 g, Ald) by a known method described in a publication (Yamanaka, M. et al., Chem. Pharm. Bull., 1991, vol. 39, p. 1556).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07470807B2 |
| Source dataset | uspto-grants-2008_12 |
| ORD ID | ord-0acf1eaf74154a6b9e3d410f310b5c29 |
| Source note | uspto-grants-2008_12 |