HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosgene → HCID 54117497, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosgene | HCID 6371 | — |
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | HCID 54132789 | HCID 54132789 | — |
| Product | HCID 54117497 | HCID 54117497 | — |
Reaction Steps
1,3-Dimethyl-3-(2-ethylhexanoylperoxy)butyl carbazate was prepared by reacting 1,3-dimethyl-3-(2-ethylhexanoylperoxy)butyl chloroformate with 11 molar excess of 54% aqueous hydrazine. 1,3-Dimethyl-3-(2-ethyl-hexanoylperoxy)butyl chloroformate was initially prepared with a purity of 72% by reacting 3-hydroxy-1,1-dimethylbutyl peroxy-2-ethylhexanoate with excess phosgene followed by removal of excess phosgene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05360867 |
| Source dataset | uspto-grants-1994_11 |
| ORD ID | ord-5515b35351cb43ec903f69b13cb50ab3 |
| Source note | uspto-grants-1994_11 |