Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Prop-2-en-1-yl bis[(prop-2-en-1-yl)oxy]acetate | HCID 18958141 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | Sodium diallyloxyacetate | HCID 5173263 | — |
Reaction Steps
21.2 g (0.1 mole) of allyl diallyloxyacetate is dissolved in 42 g of toluene then 3.92 g (98 mmoles) of sodium hydroxide dissolved in 50 g of water is introduced into this solution. This bipbase reaction medium is agitated vigorously for 30 minutes at 30° C., then decanted and the aqueous phase is collected and subjected to a vacuum distillation to eliminate the freed allyl alcohol by azeotropic distillation. The aqueous phase is then poured into acetone to precipitate the expected sodium diallyloxyacetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05360881 |
|---|
| Source dataset | uspto-grants-1994_11 |
|---|
| ORD ID | ord-6f9ae786a9ec4e03b2b3cebb29066029 |
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| Source note | uspto-grants-1994_11 |
|---|
