HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 2-(2-chloroethoxy)acetate → Methyl 2-(8-bromo-1,2,3,4,10,14b-hexahydrodibenzo[c,f]pyrazino[1,2-a]azepin-2-yl)ethoxyacetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 2-(2-chloroethoxy)acetate | HCID 15337474 | — |
| Reactant | 8-Bromo-1,2,3,4,10,14b-hexahydrodibenzo[c,f]pyrazino[1,2-a]azepine | HCID 18999756 | — |
| Product | Methyl 2-(8-bromo-1,2,3,4,10,14b-hexahydrodibenzo[c,f]pyrazino[1,2-a]azepin-2-yl)ethoxyacetate | HCID 15297699 | 38% |
Reaction Steps
Following a procedure similar to that described in Example 1, but using 8-bromo-1,2,3,4,10,14b-hexahydrodibenzo[c,f]pyrazino[1,2-a]azepine and methyl 2-chloroethoxyacetate, the title compound was obtained in a yield of 38%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05362725 |
| Source dataset | uspto-grants-1994_11 |
| ORD ID | ord-ac75c846986e4fdea12a0cb44e77df4e |
| Source note | uspto-grants-1994_11 |