HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Alcohol → Dibenzyl pyridine-2,5-dicarboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Alcohol | HCID 244 | — |
| Reactant | 2,5-Pyridinedicarboxylic acid | HCID 7493 | — |
| Solvent | Thionyl Chloride | HCID 24386 | — |
| Product | Dibenzyl pyridine-2,5-dicarboxylate | HCID 14210556 | — |
Reaction Steps
Analogously to Example 1, 20 g of pyridine-2,5-dicarboxylic acid are converted into the acid chloride with 160 ml of thionyl chloride and this is reacted with 25.9 g of benzyl alcohol. The product is recrystallized from ethyl acetate, with the addition of active charcoal.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05364873 |
| Source dataset | uspto-grants-1994_11 |
| ORD ID | ord-8ad88be545bb423d8c9bf8dff6810c1f |
| Source note | uspto-grants-1994_11 |