2,5-Pyridinedicarboxylic acid → HCID 54468594, compound

HRID 2379762Notes

Reaction equation

HRID 2379762 reaction equation
[N:1]1[CH:6]=[C:5]([C:7]([OH:9])=[O:8])[CH:4]=[CH:3][C:2]=1[C:10]([OH:12])=[O:11].[CH3:13][O:14][CH2:15][CH2:16]O>>[N:1]1[CH:6]=[C:5]([C:7]([O:9][CH2:16][CH2:15][O:14][CH3:13])=[O:8])[CH:4]=[CH:3][C:2]=1[C:10]([O:12][CH2:16][CH2:15][O:14][CH3:13])=[O:11]

Participants

3

Procedure

Analogously to Example 26, 10 g of pyridine-2,5-dicarboxylic acid are converted into the acid chloride and this is reacted with 9.1 g of ethylene glycol monomethyl ether. Working up is carried out in accordance with Example 26. The product is obtained as an oil.

Workup

  1. customThe product is obtained as an oil

Sources & evidence

ORD record
ord-20a45a442f5a4994a45530809ca6c21b
Source dataset
uspto-grants-1994_11
Patent number
US05364873

Reaction notes

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