2,5-Pyridinedicarboxylic acid → HCID 54468594, compound
Reaction equation
[N:1]1[CH:6]=[C:5]([C:7]([OH:9])=[O:8])[CH:4]=[CH:3][C:2]=1[C:10]([OH:12])=[O:11].[CH3:13][O:14][CH2:15][CH2:16]O>>[N:1]1[CH:6]=[C:5]([C:7]([O:9][CH2:16][CH2:15][O:14][CH3:13])=[O:8])[CH:4]=[CH:3][C:2]=1[C:10]([O:12][CH2:16][CH2:15][O:14][CH3:13])=[O:11]Participants
3
Procedure
Analogously to Example 26, 10 g of pyridine-2,5-dicarboxylic acid are converted into the acid chloride and this is reacted with 9.1 g of ethylene glycol monomethyl ether. Working up is carried out in accordance with Example 26. The product is obtained as an oil.
Workup
- customThe product is obtained as an oil
Sources & evidence
- ORD record
- ord-20a45a442f5a4994a45530809ca6c21b
- Source dataset
- uspto-grants-1994_11
- Patent number
- US05364873
Reaction notes
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