HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(2,4-Dichlorophenyl)-2-(1H-1,2,4-triazol-1-yl)ethanone → HCID 18956539, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(2,4-Dichlorophenyl)-2-(1H-1,2,4-triazol-1-yl)ethanone | HCID 739374 | — |
| Reactant | Lithium diisopropylamide | HCID 2724682 | — |
| Reactant | HCID 18956526 | HCID 18956526 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 18956539 | HCID 18956539 | — |
Reaction Steps
Treatment of 4-ethylpyridazine (2.16 g) with lithium diisopropylamide (0.02 mole) in dry tetrahydrofuran followed by 1-(2,4-dichlorophenyl)-2-(1H-1,2,4-triazol-1-yl)ethanone (5.12 g) according to the method of Example 9(ii) gave the title compound, diastereoisomeric pair A, (1.24 g), m.p. 174°-177°;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05364938 |
| Source dataset | uspto-grants-1994_11 |
| ORD ID | ord-d74a6ee20b194a92a44f3a6a9337a4d2 |
| Source note | uspto-grants-1994_11 |