Hydrochloric Acid → HCID 18956663, compound

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Reaction Steps

Compound [VII] (1.20 g, 1.62 mmol) was hydrogenated in CH3OH and 0.1N HCl with 10% Pd-C by the procedure used for [A]. Purification by Sephadex LH-20 column chromatography with 15% EtOH/toluene as the eluant produced 0.386 g (47%) of [A] as a colorless solid: NMR (CO3OD) δ 1.17-1.87 (m, 26H), 2.07 (s, 3H), 2.30-2.55 (m, 4H), 2.90 (t, 2H, J=6), 3.43-3.70 (m, 6H). Anal. (C23H47ClN4O6) C, H, N.

Provenance & Evidence