Thionyl Chloride → HCID 53411290, compound

HRID 2380544Notes

Reaction equation

HRID 2380544 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([CH:10]=[CH:11][CH:12]=1)[CH:5]=[CH:6][C:7](O)=[O:8].S(Cl)([Cl:15])=O>C1C=CC=CC=1>[Cl:1][C:2]1[CH:3]=[C:4]([CH:10]=[CH:11][CH:12]=1)[CH:5]=[CH:6][C:7]([Cl:15])=[O:8]

Participants

4

Reactant 2

HCID 24386Thionyl ChlorideHCID 746313-(3-Chlorophenyl)prop-2-enoic acid

Product 1

HCID 53411290HCID 53411290, compound

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

100 ml of benzene was added to 18.3 grams of m-chlorocinnamic acid. 12 ml of thionyl chloride was added dropwise slowly thereto at ambient temperature. The temperature was elevated to 80° C. and the heating was continued until foaming ceased. Benzene and thionyl chloride were distilled off and the residue was dried thoroughly under reduced pressure.

Workup

  1. customat ambient temperature
  2. customwas elevated to 80° C.
  3. distillationBenzene and thionyl chloride were distilled off
  4. customthe residue was dried thoroughly under reduced pressure

Sources & evidence

ORD record
ord-b6087c251fbd4c0c9d401ebf4cd6d338
Source dataset
uspto-grants-1994_11
Patent number
US05368737

Reaction notes

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