HCID 86745235, compound → HCID 86745234, compound

HRID 2380577Notes

Reaction equation

HRID 2380577 reaction equation
[Cl:1][CH:2]([C:7]1[CH:8]([C:28]([O:30][CH2:31][C:32]2[CH:37]=[CH:36][C:35]([N+:38]([O-:40])=[O:39])=[CH:34][CH:33]=2)=[O:29])[N:9]2[CH:12]([CH:13]=1)[CH:11]([CH:14]([O:16][C:17]([O:19][CH2:20][C:21]1[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=1)=[O:18])[CH3:15])[C:10]2=[O:27])[C:3]([O:5][CH3:6])=[O:4]>C(OCC)C>[Cl:1][C:2](=[C:7]1[CH2:13][CH:12]2[N:9]([C:10](=[O:27])[CH:11]2[CH:14]([O:16][C:17]([O:19][CH2:20][C:21]2[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=2)=[O:18])[CH3:15])[CH:8]1[C:28]([O:30][CH2:31][C:32]1[CH:33]=[CH:34][C:35]([N+:38]([O-:40])=[O:39])=[CH:36][CH:37]=1)=[O:29])[C:3]([O:5][CH3:6])=[O:4]

Participants

3

Reactant 1

HCID 86745235HCID 86745235, compound

Product 1

HCID 86745234HCID 86745234, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

The title compound is prepared by the procedure of Example 41, using 0,165 g of product from Example 42, 0,041 g (40 μl) of 1,8-diazobicyclo[5.4.0]undec-7-ene, 20 ml of diethyl ether. The organic layer is concentrated in vacuo to give 0.140 g (85%) of product as a white foam.

Workup

  1. concentrationThe organic layer is concentrated in vacuo

Sources & evidence

ORD record
ord-2b4ecf20f2cd463db943ab415f426d51
Source dataset
uspto-grants-1994_11
Patent number
US05369102

Reaction notes

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