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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2380685Generated: October 31, 2026

Tributyltin azide → HCID 178448928, compound

https://huagongshe.com/reaction/2380685

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTributyltin azideHCID 4984872—
ReactantHCID 54125536HCID 54125536—
ProductHCID 178448928HCID 178448928—

Reaction Steps

Analogously to Example 20 and using 2.2 g (5 mmol) of 2-(S)-methanesulfonylamino-3-methylbutanoic acid N-butyl-N-(2'-cyanobiphenyl-4-ylmethyl)amide and 2.5 g (7.5 mmol) of tributyltin azide, the title compound is obtained in the form of a light-coloured foam that has an Rf value of 0.45 [toluene/isopropanol/glacial acetic acid (170:30:2)].

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05369110
Source datasetuspto-grants-1994_11
ORD IDord-0ccf9135aa544e4b81fe5e3317858c5b
Source noteuspto-grants-1994_11