HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tributyltin azide → HCID 178448928, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tributyltin azide | HCID 4984872 | — |
| Reactant | HCID 54125536 | HCID 54125536 | — |
| Product | HCID 178448928 | HCID 178448928 | — |
Reaction Steps
Analogously to Example 20 and using 2.2 g (5 mmol) of 2-(S)-methanesulfonylamino-3-methylbutanoic acid N-butyl-N-(2'-cyanobiphenyl-4-ylmethyl)amide and 2.5 g (7.5 mmol) of tributyltin azide, the title compound is obtained in the form of a light-coloured foam that has an Rf value of 0.45 [toluene/isopropanol/glacial acetic acid (170:30:2)].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05369110 |
| Source dataset | uspto-grants-1994_11 |
| ORD ID | ord-0ccf9135aa544e4b81fe5e3317858c5b |
| Source note | uspto-grants-1994_11 |