Beta-Alanine → N-acryloyl-beta-alanine

HRID 2380692Notes

Reaction equation

[C:1](Cl)(=[O:4])[CH:2]=[CH2:3].[NH2:6][CH2:7][CH2:8][C:9]([OH:11])=[O:10]>>[C:1]([NH:6][CH2:7][CH2:8][C:9]([OH:11])=[O:10])(=[O:4])[CH:2]=[CH2:3]

Participants

Reactant 2

HCID 239Beta-Alanine

HCID 13140Acryloyl chloride

Product 1

HCID 324231N-acryloyl-beta-alanine

Procedure

This amide monomer was prepared from acryloyl chloride and beta-alanine per Example 1 procedure, with the recrystallized (ethyl acetate solvent) product having a melting point of 97°-99° C.

Workup

customwith the recrystallized (ethyl acetate solvent) product

Sources & evidence

ORD record: ord-bfebe56fe65c40d686ce3aad063559be
Source dataset: uspto-grants-1994_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05369142

Reaction notes

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