HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → Ethyl 4-benzyloxy-2-iodo-5-methoxybenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-Benzyloxy-2-iodo-5-methoxybenzoic acid | HCID 58345581 | — |
| Solvent | Water | HCID 962 | — |
| Product | Ethyl 4-benzyloxy-2-iodo-5-methoxybenzoate | HCID 67109995 | — |
Reaction Steps
A mixture of 4-benzyloxy-2-iodo-5-methoxybenzoic acid (reference example 5-1) (2 g), 2-iodoethane (0.5 mL), potassium carbonate (1.08 g) and N,N-dimethylformamide (17 mL) was stirred at room temperature for 2 hours. Water was added to the mixture. Insoluble materials were collected by filtration to give the title compound (2.07 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08258162B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-a4061ac4f1aa4b3d8f637ae34080fcc4 |
| Source note | uspto-grants-2012_09 |