HCID 24780974, compound → HCID 24781284, compound

HRID 2381584Notes

Reaction equation

HRID 2381584 reaction equation
[CH3:1][C:2]1[CH:14]=[C:13]([CH2:15][CH2:16][CH:17]([C:19]2[CH:24]=[CH:23][C:22]([S:25][CH3:26])=[CH:21][CH:20]=2)[OH:18])[CH:12]=[C:11]([CH3:27])[C:3]=1[O:4][C:5]([CH3:10])([CH3:9])[C:6]([OH:8])=[O:7]>C(O)CCC.O>[CH3:1][C:2]1[CH:14]=[C:13]([CH2:15][CH2:16][CH:17]([C:19]2[CH:24]=[CH:23][C:22]([S:25][CH3:26])=[CH:21][CH:20]=2)[O:18][CH2:1][CH2:2][CH2:3][CH3:11])[CH:12]=[C:11]([CH3:27])[C:3]=1[O:4][C:5]([CH3:9])([CH3:10])[C:6]([OH:8])=[O:7]

Participants

3

Reactant 1

HCID 24780974HCID 24780974, compound

Product 1

HCID 24781284HCID 24781284, compound

Reagents, catalysts & solvents 1

HCID 22253497Water butanolSolvent

Procedure

This compound was prepared following the general procedure E, using 2-[2,6-dimethyl-4-[3-[4-(methylthio)phenyl]-3-hydroxypropyl]phenoxy]-2-methylpropanoic acid in 50/50 butanol/water at 70° C. for 32 hours;

Workup

  1. customThis compound was prepared
  2. customat 70° C.
  3. customfor 32 hours

Sources & evidence

ORD record
ord-f5ba641e4a974cc8b9189881301f7d6e
Source dataset
uspto-grants-2012_09
Patent number
US08258182B2

Reaction notes

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