Iodine → HCID 421426, compound

HRID 2382296Notes

Reaction equation

[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([NH2:9])=[CH:5][CH:4]=1.II.O=[C:13]([CH:15]=[C:16]([CH3:18])[CH3:17])[CH3:14]>>[CH3:1][O:2][C:3]1[CH:8]=[C:7]2[C:6](=[CH:5][CH:4]=1)[NH:9][C:16]([CH3:18])([CH3:17])[CH:15]=[C:13]2[CH3:14]

Participants

Reactant 3

HCID 807Iodine

HCID 7732P-Anisidine

HCID 8858Mesityl oxide

Product 1

HCID 421426HCID 421426, compound

Procedure

Skraup reaction of 4-anisidine (5.0 g) and iodine (1.7 g) in mesityl oxide (25 ml) was performed according to the method described in example 1.

Sources & evidence

ORD record: ord-1edf182d86f146c0b0e72e5e003d37ae
Source dataset: uspto-grants-2012_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08258293B2

Reaction notes

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