HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,3-Dimethylbutanoyl chloride → HCID 66992471, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,3-Dimethylbutanoyl chloride | HCID 81514 | — |
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | HCID 17962881 | HCID 17962881 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 66992471 | HCID 66992471 | — |
Reaction Steps
Acylation of 1-acetyl-6-hydroxy-4-phenyl-1,2,3,4-tetrahydro-2,2,4-trimethylquinoline (10 mg) with tert-butylacetyl chloride (9.0 l) and N,N-diisopropylethylamine (28 l) in tetrahydrofuran (1 ml) was performed according to the method described in example 6.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08258293B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-1b67c24d5c404df3b2d8ae24a21d7212 |
| Source note | uspto-grants-2012_09 |