HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphenylphosphine → HCID 17962936, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | Cesium fluoride | HCID 25953 | — |
| Reactant | 1,1'-Biphenyl-4-yl-boronic acid | HCID 151253 | — |
| Reactant | HCID 17962933 | HCID 17962933 | — |
| Catalyst | Bis(dibenzylideneacetone)palladium | HCID 9811564 | — |
| Solvent | Dimethoxyethane ethanol | HCID 20074477 | — |
| Product | HCID 17962936 | HCID 17962936 | — |
Reaction Steps
Suzuki cross-coupling of 1-acetyl-6-iodo-4-phenyl-1,2,3,4-tetrahydro-2,2,4-trimethylquinoline (20 mg), (1,1′-biphenyl-4-yl)boronic acid (28 mg), cesium fluoride (15 mg), triphenylphosphine (5 mg) and tris(dibenzylideneacetone)dipalladium(0) (4.5 mg) in dimethoxyethane/ethanol 4:1 (v/v) (5 ml) was performed according to the method described in example 13.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08258293B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-e3e0adc9f36b44bca6e2144e0e2be6d5 |
| Source note | uspto-grants-2012_09 |