Calcium Hydroxide → Calcium phenolsulfonate

HRID 2382505Notes

Reaction equation

HRID 2382505 reaction equation
[CH:1]1[CH:6]=[CH:5][C:4]([OH:7])=[CH:3][CH:2]=1.[OH:8][S:9]([O-:11])=[O:10].[OH-].[Ca+2:13].[OH-]>>[CH:5]1[C:4]([OH:7])=[CH:3][CH:2]=[C:1]([S:9]([O-:11])(=[O:10])=[O:8])[CH:6]=1.[CH:5]1[C:4]([OH:7])=[CH:3][CH:2]=[C:1]([S:9]([O-:11])(=[O:10])=[O:8])[CH:6]=1.[Ca+2:13]

Participants

3

Reactant 2

HCID 6093208Calcium HydroxideHCID 53433159HCID 53433159, compound

Product 1

HCID 31392Calcium phenolsulfonate

Procedure

While 1000 g of a phenol sulfonic acid aqueous solution at a concentration of 5% was stirred at room temperature, calcium hydroxide was gradually added to reach a pH of about 6. The mixture was continuously stirred for a while. Then, this was filtered with 0.4 micrometer glass filter to obtain a calcium phenolsulfonate aqueous solution, which was then spray-dried to obtain powders of calcium phenolsulfonate.

Workup

  1. filtrationThen, this was filtered with 0.4 micrometer glass
  2. filtrationfilter

Sources & evidence

ORD record
ord-d8a40513c593473aaea79664c630fdc0
Source dataset
uspto-grants-2012_09
Patent number
US08262941B2

Reaction notes

Loading…