Water → HCID 16662056, compound

Participants

Reaction Steps

In a 25 ml round-bottom flask 0.085 p-anisoyl chloride and 0.04 mL of pyridine are dissolved in 3 ml of MTBE. To this solution was added 0.10 g of 2-(2-anilinoethyl)pyridine. The solution is stirred at room temperature for 24 h. To the solution was added 5 mL of water. The organic layer was separated and washed with 5 mL of water. The organic layer was dried over MgSO4. The solvent was evaporated to yield a brown oil. The oil was purified on silica gel to afford 0.15 g of an off-white solid with the following spectroscopic properties:

Provenance & Evidence