Ethyl chloroformate → HCID 58288713, compound

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Reaction Steps

Prepared from 3,5-diisopropylbenzene-1,2-diol and ethyl chloroformate; purified by flash column chromatography on silica gel to yield a yellow oil (59.1%); 1H NMR (500 MHz, CDCl3, ppm) δ 7.02 (s, 1H), 6.98 (s, 1H), 4.32 (q, 2H, J=7.0 Hz), 4.31 (q, 2H, J=7.0 Hz), 3.11 (heptat, 1H, J=7.3 Hz), 2.89 (heptat, 1H, J=7.0 Hz), 1.38 (t, 3H, J=7.3 Hz), 1.37 (t, 3H, J=7.0 Hz), 1.24 (d, 6H, J=7.0 Hz), 1.22 (d, 6H, J=7.5 Hz).

Provenance & Evidence