tert-Butoxy bis(dimethylamino)methane → HCID 68744373, compound

HRID 2382597Notes

Reaction equation

HRID 2382597 reaction equation
[O:1]1[C:5]2[CH:6]=[CH:7][C:8]([NH:10][S:11]([C:14]3[CH:19]=[C:18]([CH2:20][C:21](=[O:23])[CH3:22])[CH:17]=[CH:16][C:15]=3[Cl:24])(=[O:13])=[O:12])=[CH:9][C:4]=2[O:3][CH2:2]1.C(O[CH:30](N(C)C)[N:31]([CH3:33])[CH3:32])(C)(C)C>>[O:1]1[C:5]2[CH:6]=[CH:7][C:8]([NH:10][S:11]([C:14]3[CH:19]=[C:18](/[C:20](=[CH:30]\[N:31]([CH3:33])[CH3:32])/[C:21](=[O:23])[CH3:22])[CH:17]=[CH:16][C:15]=3[Cl:24])(=[O:13])=[O:12])=[CH:9][C:4]=2[O:3][CH2:2]1

Participants

3

Reactant 2

HCID 79885tert-Butoxy bis(dimethylamino)methaneHCID 68725025HCID 68725025, compound

Product 1

HCID 68744373HCID 68744373, compound

Procedure

This compound is prepared analogously to Example 1-39 by replacing 2-Chloro-N-(3-cyano-phenyl)-5-(2-oxo-propyl)-benzenesulfonamide with N-Benzo[1,3]dioxol-5-yl-2-chloro-5-(2-oxo-propyl)-benzenesulfonamide and by replacing N,N-dimethylformamide dimethyl acetyl with t-butoxy-bis(dimethylamino) methane to afford the title compound.

Workup

  1. customThis compound is prepared analogously to Example 1-39

Sources & evidence

ORD record
ord-d4b335c3e4444486a0ccfebd252fdbf0
Source dataset
uspto-grants-2012_09
Patent number
US08263585B2

Reaction notes

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