HRID2382631

反应详情

EQUATION

反应方程式

HRID 2382631 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

CONDITIONS

反应条件

温度
61 °C

PROCEDURE

实验过程

2,4-Dichloro-5-nitro-pyrimidine (1.94 g, 10 mmol) and 2-amino-N-methyl-benzenesulfonamide (1.86 g, 10 mmol) are dissolved in CHCl3 (30 mL). The reaction mixture is heated at 61° C. for 2 h. The solvent is evaporated and the residue is washed with ether to give the title product.

WORKUP

后处理

  1. customThe solvent is evaporated
  2. washthe residue is washed with ether