2,4-Dichloro-5-nitropyrimidine → HCID 58748430, compound

Participants

Role	Name	HCID	Charge
Reactant	2,4-Dichloro-5-nitropyrimidine	HCID 521266	—
Reactant	2-amino-N-methylbenzene-1-sulfonamide	HCID 1132840	—
Solvent	Chloroform	HCID 6212	—
Product	HCID 58748430	HCID 58748430	—

Reaction Conditions

Temperature	61 °C

Reaction Steps

2,4-Dichloro-5-nitro-pyrimidine (1.94 g, 10 mmol) and 2-amino-N-methyl-benzenesulfonamide (1.86 g, 10 mmol) are dissolved in CHCl3 (30 mL). The reaction mixture is heated at 61° C. for 2 h. The solvent is evaporated and the residue is washed with ether to give the title product.

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US08263590B2
Source dataset	uspto-grants-2012_09
ORD ID	ord-d90498611c7e45f2a91915b7a8ec408a
Source note	uspto-grants-2012_09