HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Anisoyl chloride → N-[5-(3-furyl)[1,2,4]triazolo[1,5-a]pyridin-2-yl]-4-methoxybenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Anisoyl chloride | HCID 7477 | — |
| Reactant | 5-(Furan-3-yl)-[1,2,4]triazolo[1,5-a]pyridin-2-amine | HCID 25215938 | — |
| Product | N-[5-(3-furyl)[1,2,4]triazolo[1,5-a]pyridin-2-yl]-4-methoxybenzamide | HCID 25213271 | — |
Reaction Steps
The title compound was prepared following procedure and work up described for example 19, but starting from 5-(3-furyl)[1,2,4]triazolo[1,5-a]pyridin-2-amine ((A2), 50 mg; 0.25 mmol; 1.0 eq.) and p-anisoyl chloride (66 mg; 0.50 mmol; 2.0 eq.) as a white powder (58.2 mg, 69%). HPLC, Rt: 3.19 min. (purity 97.0%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08263595B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-752c119e141448d2a8d7ee9b2d9e4dcb |
| Source note | uspto-grants-2012_09 |