2,3-dihydro-1,4-benzodioxine-6-carbonyl chloride → HCID 25213507, compound

Participants

Reaction Steps

The title compound was prepared following procedure and work up described for example 19, but starting from 5-(3-furyl)[1,2,4]triazolo[1,5-a]pyridin-2-amine ((A2), 50 mg; 0.25 mmol; 1.0 eq.) and 2,3-dihydro-1,4-benzodioxine-6-carbonyl chloride (74 mg; 0.37 mmol; 1.5 eq.) as a white powder (34 mg, 37%). HPLC, Rt: 3.17 min. (purity 81.5%). LC/MS, M+(ESI): 363.0.

Provenance & Evidence