4-Hydroxyphenylboronic acid → N-[6-(4-hydroxyphenyl)[1,2,4]triazolo[1,5-a]pyridin-2-yl]benzamide

Participants

Reaction Steps

The title compound was prepared following procedure described for example 56 but starting from N-(6-bromo[1,2,4]triazolo[1,5-a]pyridin-2-yl)benzamide ((B5), 150 mg; 0.47 mmol; 1.0 eq.) and 4-hydroxyphenylboronic acid (131 mg; 0.95 mmol; 2.0 eq.) as a white solid (15 mg, 9%). HPLC, Rt: 2.60 min. (purity 97.2%). LC/MS, M+(ESI): 331.1, M−(ESI): 329.1.

Provenance & Evidence