Hydrochloric Acid → HCID 67536266, compound

Participants

Reaction Steps

The title compound was prepared following procedure described for example 56 but starting from N-(6-bromo[1,2,4]triazolo[1,5-a]pyridin-2-yl)nicotinamide ((B6), 400 mg; 1.26 mmol; 1.0 eq.) and 2-methoxy-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenol (629 mg; 2.51 mmol; 2.0 eq.) as a light yellow solid (249 mg, 55%). HPLC, Rt: 1.71 min. (purity 60.7%). LC/MS, M+(ESI): 362.0, M−(ESI): 360.0. CHN analysis: [C19H15N5O3.1 HCl.0.4 CH3CN.0.6H20] Corrected: C, 55.95%; H, 4.36%; N, 17.79%. Found: C, 55.95%; H, 4.76%; N, 17.53%.

Provenance & Evidence