HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexanemethylamine → HCID 25214731, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexanemethylamine | HCID 76688 | — |
| Reactant | HCID 25212520 | HCID 25212520 | — |
| Product | HCID 25214731 | HCID 25214731 | — |
Reaction Steps
The title compound was prepared following procedure described for example 76 but starting from N-[5-chloro-7-(trifluoromethyl)[1,2,4]triazolo[1,5-a]pyridin-2-yl]nicotinamide ((B7), 50 mg; 0.14 mmol; 1.0 eq.) and cyclohexanemethylamine (500 μl) as a white powder (27 mg; 44%). HPLC, Rt: 4.11 min. (purity 99.8%). LC/MS, M+(ESI): 419.4, M−(ESI): 417.4.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08263595B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-a6a4acaab80c4dd080018f227b52b855 |
| Source note | uspto-grants-2012_09 |