HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-tert-Butylcyclohexylamine → HCID 59437467, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-tert-Butylcyclohexylamine | HCID 79396 | — |
| Reactant | N-(5-chloro[1,2,4]triazolo[1,5-a]pyridin-2-yl)nicotinamide | HCID 25212516 | — |
| Product | HCID 59437467 | HCID 59437467 | — |
Reaction Steps
The title compound was prepared following procedure and work up described for example 79 but starting from N-(5-chloro[1,2,4]triazolo[1,5-a]pyridin-2-yl)nicotinamide ((B4), 80 mg; 0.29 mmol; 1.0 eq.) and 4-tert-butylcyclohexylamine (91 mg; 0.58 mmol; 2.0 eq.) as a white powder (32 mg, 27%). HPLC, Rt: 4.63 min. (purity 99.3%). LC/MS, M+(ESI): 393.1, M−(ESI): 391.1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08263595B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-7bda01324f444b6387899a14036cb06c |
| Source note | uspto-grants-2012_09 |