HRID2382996

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID6790

4-Amino-1-naphthalenesulfonic acid

C10H9NO3S

结构：O=S(=O)(O)c1cc(NC2=CC(Cl)=NN(Cl)N2)ccc1C=Cc1ccc(NC2=CC(Cl)=NN(Cl)N2)cc1S(=O)(=O)O

HCID178527627

未命名化合物

PRODUCTS

生成物

结构：O=S(=O)(O)c1cc(NC2=CC(Nc3ccc(S(=O)(=O)O)c4ccccc34)=NN(Cl)N2)ccc1C=Cc1ccc(NC2=CC(Nc3ccc(S(=O)(=O)O)c4ccccc34)=NN(Cl)N2)cc1S(=O)(=O)O

HCID86623307

未命名化合物

CONDITIONS

反应条件

温度: 20 °C

PROCEDURE

实验过程

An aqueous solution of 1-aminonaphthalene-4-sulfonic acid (0.012 mol) was added to the freshly produced solution according to Example 4 of 4,4′-bis-(2,4-dichlorotriazin-6-ylamino)-stilbene-2,2′-disulfonic acid (0.006 mol). The mixture was stirred at pH 5.5 and 20° C. for 24 hours.

来源与证据

来源类型: Open Reaction Database
ORD 记录: ord-9b109db2a95e4056a04db94055af2c81
来源数据集: uspto-grants-2012_09
DOI: 10.6084/m9.figshare.5104873.v1
专利: US08263541B2
来源说明: uspto-grants-2012_09

反应 SMILES

[NH2:1][C:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[C:5]([S:12]([OH:15])(=[O:14])=[O:13])=[CH:4][CH:3]=1.[Cl:16][N:17]1[N:22]=[C:21](Cl)[CH:20]=[C:19]([NH:24][C:25]2[CH:26]=[C:27]([S:52]([OH:55])(=[O:54])=[O:53])[C:28]([CH:31]=[CH:32][C:33]3[C:34]([S:48]([OH:51])(=[O:50])=[O:49])=[CH:35][C:36]([NH:39][C:40]4[NH:45][N:44]([Cl:46])[N:43]=[C:42](Cl)[CH:41]=4)=[CH:37][CH:38]=3)=[CH:29][CH:30]=2)[NH:18]1>>[Cl:16][N:17]1[N:22]=[C:21]([NH:1][C:2]2[C:11]3[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=3)[C:5]([S:12]([OH:15])(=[O:13])=[O:14])=[CH:4][CH:3]=2)[CH:20]=[C:19]([NH:24][C:25]2[CH:26]=[C:27]([S:52]([OH:55])(=[O:54])=[O:53])[C:28]([CH:31]=[CH:32][C:33]3[C:34]([S:48]([OH:51])(=[O:50])=[O:49])=[CH:35][C:36]([NH:39][C:40]4[NH:45][N:44]([Cl:46])[N:43]=[C:42]([NH:1][C:2]5[C:11]6[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=6)[C:5]([S:12]([OH:15])(=[O:13])=[O:14])=[CH:4][CH:3]=5)[CH:41]=4)=[CH:37][CH:38]=3)=[CH:29][CH:30]=2)[NH:18]1