Bromine → HCID 59591080, compound

Participants

Reaction Steps

Bromine (2.38 g; 14.9 mmol) in dichloromethane (10 ml) was added to a solution of {2-[2-methyl-3-(methyloxy)phenyl]ethyl}amine (Preparation 10; 2.73 g; 16.52 mmol) in dichloromethane (150 ml) over 3 min at 0° C. Removal of the solvent, trituration with diethyl ether, filtration and drying under vacuum gave the title compound (4.17 g) as a pale orange solid.

Provenance & Evidence