Acetophenone → HCID 72535740, compound

HRID 2383355Notes

Reaction equation

HRID 2383355 reaction equation
[I:1][C:2]1[CH:7]=[CH:6][C:5]([NH:8][NH2:9])=[CH:4][C:3]=1[CH3:10].[C:11]([C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1)(=O)[CH3:12]>>[I:1][C:2]1[CH:7]=[CH:6][C:5]([NH:8][N:9]=[C:11]([C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)[CH3:12])=[CH:4][C:3]=1[CH3:10]

Participants

3

Reactant 2

HCID 7410AcetophenoneHCID 57436927HCID 57436927, compound

Product 1

HCID 72535740HCID 72535740, compound

Procedure

Analogously to the process described under Example 1A, 992 mg (4.0 mmol) of the compound from Example 6A and 721 mg (6.0 mmol) of acetophenone give 1.405 g (100% of theory) of the title compound.

Sources & evidence

ORD record
ord-a834b36bcbdd4009aaff10bcc3e63fa0
Source dataset
uspto-grants-2012_09
Patent number
US08263624B2

Reaction notes

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