Phenyl isocyanate → HCID 59490494, compound

Participants

Reaction Steps

The compound N-phenyl-6,7-dihydropyrazolo[4′,3′:5,6]pyrido[3,4-d][1]benzazepine-8(3H)-carboxamide was prepared using 3-(4-methoxybenzyl)-3,6,7,8-tetrahydropyrazolo[4′,3′:5,6]pyrido[3,4-d][1]benzazepine and phenyl isocyanate as described in the two step general procedure L to give the desired compound as an off-white solid (0.048 g, 31%). M.p.>140° C.; 1H NMR (CDCl3, 400 MHz) δ 11.35 (brs, 1H), 8.08 (s, 1H), 8.00 (s, 1H), 7.99 (m, 1H), 7.68-7.60 (m, 2H), 7.46 (dd, J1=1.6 Hz, J2=7.2 Hz, 1H), 7.15-7.06 (m, 4H), 6.90 (m, 1H), 5.97 (s, 1H), 4.75 (m, 1H), 3.77 (m, 1H), 2.90 (m, 2H); LCMS [M+H]: 356.

Provenance & Evidence