HRID238359

反应详情

EQUATION

反应方程式

HRID 238359 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

10% Palladium carbon (30 mg) was added to an ethanol (3.0 mL) solution of 1-methyl-5-(2-phenylethenyl)-1H-pyrazole (300 mg), and the obtained solution was then stirred under a hydrogen atmosphere at a room temperature for 14 hours. Thereafter, the reaction solution was filtrated with Celite, and the filtrate was then concentrated under a reduced pressure, so as to obtain the title compound (310 mg) in the form of a colorless oily substance.

WORKUP

后处理

  1. filtrationThereafter, the reaction solution was filtrated with Celite
  2. concentrationthe filtrate was then concentrated under a reduced pressure