HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dicyclohexylamine → HCID 57883903, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dicyclohexylamine | HCID 7582 | — |
| Reactant | HCID 43409799 | HCID 43409799 | — |
| Reactant | HCID 86611180 | HCID 86611180 | — |
| Product | HCID 57883903 | HCID 57883903 | — |
Reaction Steps
[2-(3,3-Dicyclohexyl-ureido)-thiazol-4-ylmethylsulfanyl]-acetic acid ethyl ester prepared as described in general procedure (A) using dicyclohexylamine and (2-amino-thiazol-4-ylmethylsulfanyl)-acetic acid ethyl ester (prepared by reaction of 4-chloromethyl-thiazol-2-ylamine, ethyl-2-mercaptoacetate and potassium carbonate in DMF for 1 h at room temperature). Hydrolysis using general procedure (F) gave the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08263634B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-a4bc7e74a63c40e782027226ac7fd0e4 |
| Source note | uspto-grants-2012_09 |