HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylaziridine → HCID 58210218, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylaziridine | HCID 6377 | — |
| Reactant | 3-(Acryloyloxy)-2-hydroxypropyl methacrylate | HCID 5062351 | — |
| Product | HCID 58210218 | HCID 58210218 | 99.3% |
Reaction Steps
To a 250 mL round bottomed flask were added 3-(acryloyloxy)-2-hydroxypropyl methacrylate (32.1 g, 0.15 mol, available from Aldrich) and 2-methylaziridine (10.8 g, about 0.17 mol, 90% pure, available from Aldrich) to cause a slight exotherm. The reaction mixture was allowed to stand at room temperature overnight. Excess 2-methylaziridine was removed at reduced pressure to leave the desired product (40.4 g) as a colorless liquid. NMR and IR spectral analyses confirmed the structure of the product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08263711B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-fe4a23c060964785adf49068dc0aab77 |
| Source note | uspto-grants-2012_09 |