HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Methylaniline → HCID 25104176, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Methylaniline | HCID 7515 | — |
| Reactant | 2,1,3-Benzoxadiazole-5-carbonyl chloride | HCID 2735453 | — |
| Product | HCID 25104176 | HCID 25104176 | — |
Reaction Steps
Prepared from N-methylaniline and [2,1,3]-benzoxadiazole-5-carbonylchloride using the procedure described for Example 7. N-Methyl-N-phenyl-[2,1,3]-benzoxadiazole-5-carboxamide was isolated as a yellow oil. LC-MS, MH+=254; 1H NMR (300 MHz, CDCl3) δ 7.74 (s, 1H); 7.64 (d, 1H, J=9.6 Hz); 7.34 (d, 1H, J=9.6 Hz); 7.29-7.09 (m, 5H); 3.54 ppm (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08642633B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-f43de5666dd848c493c77aba89d0edb2 |
| Source note | uspto-grants-2014_02 |